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Sprey döküm nanoyapılı CdS ince filmlerinin bazı fiziksel özellikleri üzerine tavlama sıcaklığının etkisi

The influence of annealing temperature on some physical properties of spray deposited nanostructured CdS thin films

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DOI: 
http://dx.doi.org/10.17776/csj.69365

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Abstract (2. Language): 
In this study, the effect of annealing temperature on physical properties of CdS thin films was studied. CdS in the form of thin film was prepared by a simple and inexpensive spray pyrolysis technique for various annealing temperatures. After deposition, films were annealed at 400-450-500 °C for 2 hours at air atmosphere. The effects of the annealing temperature on the physical properties of the films were investigated by studying the transmittance measurements, spectroscopic ellipsometry technique, atomic force microscope (AFM) observations and the four probe technique. The transmittance measurements were used to estimate the band gap energy by the linear fit of (h)2 curve. The band gap energy was found to be slightly decreasing with the annealing process. From the four probe measurement the resistivity was determined and found to be strongly decreasing with increasing the annealing temperature. Finally, annealing process and annealing temperature confirmed significant effects on the optical, electrical and surface properties CdS thin films.
Abstract (Original Language): 
Bu çalışmada, CdS ince filmlerin fiziksel özellikleri üzerine tavlama sıcaklığının etkisi çalışıldı. İnce film formundaki CdS, basit ve pahalı olmayan sprey piroliz yöntemiyle, çeşitli tavlama sıcaklıklarında hazırlandı. Çökelme sonrası, filmler hava atmosferinde 2 saat boyunca 400-450-500 oC’de tavlandı. Geçirgenlik ölçümleri, spektroskopik elipsometre tekniği, atomik kuvvet mikroskobu (AFM) gözlemleri ve dört uç tekniği çalışmalarıyla, filmlerin fiziksel özellikleri üzerine tavlama sıcaklığının etkisi incelendi. Geçirgenldoğrusal fitleme ile, band aralığı tahminlerinde kullanıldı. Band aralık enerjisinin, tavlama süreci ile hafifçe azaldığı bulundu. Dört uç ölçümlerinden, direnç belirlendi ve artan tavlama sıcaklığı ile hızla azaldığı görüldü. Son olarak, tavlama süreci ve tavlama sıcaklığının CdS ince filmlerin optik, elektrik ve yüzey özellikleri üzerinde önemli etkileri doğruladı.
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REFERENCES

References: 

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The influence of annealing temperature on some physical properties of spray deposited
nanostructured CdS thin films
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