Buradasınız

MİKRODALGA ENERJİSİNİN ANALİTİK KİMYA SAHASINDA VE KATALİZÖR HAZIRLAMADA KULLANIMI

THE USAGE OF MICROWAVE ENERGY IN ANALYTICAL CHEMISTRY AREA AND PREPERATION OF CATALYSIS

Journal Name:

Publication Year:

Abstract (2. Language): 
In this article, microwave energy, because of its excellent properties, has been used in the analytical chemistry applications such as sample digestion, solvent extraction, sample drying, the measurement of moisture, analyt desorption and adsorption, sample clean-up, chromogenic reaction, speciation and nebulization of analytical samples, the effect of microwaves on catalysis preperation used in industry, the hypotesis and the ideas written on this matter and the examples concerned with the practice exercise into the preperation of catalysis were submitted. The important developments used into the analytical chemistry and the prepare of catalysis area in the latest years was appreciated and taked aim at the academician studied on this subjects.
Abstract (Original Language): 
Bu makalede, mikrodalga enerjisinin, sahip olduğu üstün özelliklerinden dolayı, analitik kimya sahasında sıklıkla karşılaşılan numune çözündürme, çözücü ekstraksiyonu, numune kurutma, nem ölçümü, çözücü desorbsiyonu -absorbsiyonu, numune temizleme, khromogenik reaksiyonlar, analitik numunelerin analize hazırlanması ve nebulizasyon konularına ve ayrıca endüstride kullanılan katalizörler hazırlanırken mikrodalgaların kullanılması sonucu ortaya çıkan etkilere, ortaya konan hipotezlere, ileri sürülen görüşlere yer verilmiş ve katalizör hazırlama safhalarında kullanımı ile ilgili uygulamalardan örnekler sunulmuştur. Bu çalışma ile, mikrodalga enerjisinin analitik kimya sahasında ve katalizör hazırlamadaki kullanım tekniklerine yönelik olarak son yıllarda ortaya çıkan önemli gelişmeler değerlendirilmiş ve böylece bu konularda çalışan akademisyenlere katkıda bulunulması hedef alınmıştır.
262
277

REFERENCES

References: 

Anonymous, 1998. Proceedings of International Conference on Microwave Chemistry, Institute of Chemical Process Fundamentals, Academy of Sciences of Czech Republic, Prague, Czech Republic.
Anonymous, 2000. Proceedings of International Conference on Microwave Chemistry, Association for Microwave Power in Europe for Resarch ve Education, Antibes, France.
Anonymous, 2001. Book of Abstract, 8th International Conference on Microwave ve High
Frequency Heating, Bayreuth, Germany.
Arafat, A., Jansen, J., Ebaid, A. and Vanbekkum, H. 1993. Microwave Preparation of Zeolite-Y and Zsm-5. Zeolites. (13), 162-165.
Baysar, A. and Kuester, L. 1994. Mikrodalgalarla Isıtılan Akışkan Yataklı Reaktörlerde Saf Silisyum Üretimi. 1.Ulusal Kimya Mühendisliği Kongre Kitabı, 13-16 Eylül 1994. Ankara. (1), 528-537.
Bond, G., Moyes, R., Pollington, S. and Whan, D. 1993a. The Advantageous Use of Microwave-Radiation in the Treparation of Supported Nickel-Catalysts. Studies in Surface Science ve Catalysis.
(75), 1805-1808.
Bond, G., Moyes, R. and Whan, D. 1993b. Recent Applications of Microwave - Heating in Catalysis.
Catalysis Today. (3), 427-437.
Breccia, A., Esposito, B., Fratadocchi, G. and Fini, A. 1999. Reaction Between Methanol and Commercial Seed Oils under Microwave Irradiation. Journal of Microwave Power ve Electromagnetic
Energy. (34), 3-8.
Burguera, J., Carrero, P., Burguera, M., Rondon, C., Brunetto, M. and Gallignani, M. 1996. Flow Injection for the Determination of Se(IV) and Se(VI) by Hydride Generation Atomic Absorption Spectrometry with Microwave Oven On-Line Prereduction of Se(VI) To Se(IV). Spectrochimica Acta Part B-Atomic Spectroscopy. (51), 1837-1847.
Brook, S.L., Marquez, M., Suib, S.L., Hayashi, Y. and Matsumoto, H. 1998. Plasma Decomposition of CO2 in the Presence of Metal Catalysts. Journal of
Catalysis. (180), 225-233.
Chee, K., Wong, M. and Lee, H. 1996.
Determination of Organochlorine Pesticides in Water by Membranous Solid-Phase Extraction, and in Sediment by Microwave-Assisted Solvent Extraction with Gas Chromatography and Electron-Capture and Mass Spectrometric Detection. Journal of Chromatography A. (736), 211-218.
Donard, O., Lalere, B. and Martin, F. 1995.
Microwave-Assisted Leaching of Organotin Compounds from Sediments for Speciation Analysis.
Analytical Chemistry. (67), 4250-4254.
Galema, S.A. 1997. Microwave Chemistry, Chem.
Soc. Rev. 26, 233-238.
Hajek, M., Radoiu, M. 2000. Microwave Activation of Catalytic Transformation of Tutylphenols. Journal of Molecular Catalysis A - Chemical.
(2), 383-392.
Hajek, M. 1997. Microwave Activation of Homogeneous and Heterogeneous Catalytic
Mühendislik Bilimleri Dergisi 2008 14 (3) 267-277
276
Journal of Engineering Sciences 2008 14 (3) 267-277
Mikrodalga Enerjisinin Analitik Kimya Sahasında ve Katalizör Hazırlamada Kullanımı, S. Kuşlu, F. Çavuş
Reactions. Collection of Czechoslovak Chemical Communications. (2), 347-354.
Jin, Q.H., Shi, Y., Yu, A., Yang, W.J. and Peng, Z. 1999. An Improved Argon Microwave-Induced Plasma Ionization Detector for Gas Chromotograp.
Microchemical Journal. (62), 282-290.
Jacob, J., Chia, H.L. and Boey, F.C. 1995. Rewiev Thermal ve Non-Thermal Interaction of Microwave Radiation with Materials. Journal of Materials
Science. (30), 5321-5327.
Kingston, H. and Haswell, J. 1997. Microwave -Enhanced Chemistry, Fundamentals, Sample Preperation and Applications, 774 p. American Chemical Society. Washington, DC.
Koropchak, J. and Veber, M. 1992. Thermospray Sample Introduction to Atomic Spectrometry. Critical Reviews in Analytical Chemistry. (23),
113-141.
Langa, F., Cruz, P.L., De La Hoz, A., Ortiz, A.D. and Barra, E.D. 1996. Microwave Irradiation: More Than Just a Method for Accelerating Reactions. Contemporary Organic Synthesis. 373-386.
Mahan, K., Foderaro, T., Garza, T., Martinez, R., Maroney, G., Trivisonno, M. and Willging, E. 1987. Microwave Digestion Techniques in the Sequential Extraction of Calcium, Iron, Chromium, Manganese, Lead, ve Zinc in Sediments. Analytical Chemistry.
(59), 938-945.
Oktay, A., Akın, O. ve Oğuz, A. 1999. Seramiklerin Mikrodalga Enerjisi ile Kurutulması ve Sinterlenmesi. Elektrik Mühendisliği 6. Ulusal Kongre Kitabı, 11-17 Eylül, 1999. Bursa. 672- 675.
Onuska, F. and Terry K. 1995. Microwave Extraction in Analytical-Chemistry of Pollutants -Chlorinated Benzenes. Journal of Microcolumn
Separations. (7), 319-326.
Prasad, N., Yeh H., Adler R., Tao, W. 1995.
Microwave ve Infrared Simulations of an Intense
Convective System and Comparison with Aircraft Observations, Journal of Applied Meteorology. (34), 153-174.
Pawlicka, A., Pereira, C., Nascimento, O., Bulhoes, L. and Walmsley, L. 1997. Metal-insulator transitions in pressed pellets of BF4- doped poly (3ethylthiophene). Phase Transitions. Part A.
(62), 157-165.
Ringler, S., Girard, P., Maire, G., Hilaire, S., Roussy, G. and Garin, F. 1999. Mechanistic Studies of NOx Reduction Reactions Under Oxidative Atmosphere on Alumina Supported 0.2wt % Platinum Catalyst Treated under Microwave (Part II). Applied Catalysis B-Environmental.
(20), 219-233.
Roussy, G., Marchal, E., Thiebaut, J., Kiennemann, A. and Maire, G. 1997. C-2(+)Selectivity Enhancement in Oxidative Coupling of Methane over Microwave-Irradiated Catalysts. Fuel Processıng Technology. (50), 261-274.
Smith, F. and Arsenault, E. 1996. Microwave-Assisted Sample Preparation in Analytical
Chemistry. Talanta. (43), 1207-1268.
Strauss, C.R. and Trainor, R.W. 1995. Invited
Review Development in Microwave-Assisted
Organic Chemistry. Aust. J. Chem. (48), 1665-1669.
Taner, P. and Leong, L. 1997. Microwave Vacuum Drying of Marine Sediment: Determination of Moisture Content, Metals and Total Carbon.
Analytica Chimica Acta. (342), 247-252.
Tse, M., Depew, M. and Wan J. 1990. Applications of High Power Microwave Catalysis in Chemistry. Research on Chemical Intermediates. (13), 221-236.
Wan, J., Sauren, H., Wren, J. and Pemberton, R. 1993. Microwave-Induced Acoustic Phenomenon- A Potential Analytical Sensor for Ionic Conducting Materials in Aqueous and Organic Media. Spectroscopy Letters. (26), 1231-1240 .

Thank you for copying data from http://www.arastirmax.com